Crystal structure and Hirshfeld surface analysis of 3-(hydroxymethyl)-3-methyl-2,6-diphenylpiperidin-4-one

Crystal structure and Hirshfeld surface analysis of 3-(hydroxymethyl)-3-methyl-2,6-diphenylpiperidin-4-one

A new synthesis of the title compound, C19H21NO2, was developed with good yield and purity using the reaction of 4-hydroxy-3-methyl-2-butanone, benzaldehyde and ammonium acetate in glacial acetic acid as a solvent. The central piperidine ring adopts a chair conformation, and its least-squares basal...

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Bibliographic Details
Main Authors: Mustafa Kemal Gümüş, Sevgi Kansiz, Gulzhamal Bagitovna Tulemisova, Necmi Dege, Eiad Saif
Format: Article
Language:English
Published: International Union of Crystallography 2022-01-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
piperidone
benzaldehyde
4-hydroxy-3-methyl-2-butanone
ammonium acetate
hirshfeld surface
hydrogen bonding
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989021012640

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http://scripts.iucr.org/cgi-bin/paper?S2056989021012640

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