From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process Simulations
New product development for distilled spirits frequently involves experimental trials at the laboratory scale that attempt to replicate industrial-scale production processes. This process is time-consuming and limits the number of samples that can be analysed. The aim of the present study was to con...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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MDPI AG
2023-04-01
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| Series: | Beverages |
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| Online Access: | https://www.mdpi.com/2306-5710/9/2/37 |
| _version_ | 1827738553929433088 |
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| author | Martina Daute Irene Baxter Barry Harrison Graeme Walker Frances Jack |
| author_facet | Martina Daute Irene Baxter Barry Harrison Graeme Walker Frances Jack |
| author_sort | Martina Daute |
| collection | DOAJ |
| description | New product development for distilled spirits frequently involves experimental trials at the laboratory scale that attempt to replicate industrial-scale production processes. This process is time-consuming and limits the number of samples that can be analysed. The aim of the present study was to conduct laboratory-scale Scotch malt whisky production experiments to determine if samples taken from earlier in the production process, that is, directly after fermentation (wash stage) or after a single distillation (low wines stage), showed similar analytical differentiation compared to samples of fresh distillates (new make spirits). Napping, a rapid sensory method, was used to assess the impact on flavour characteristics while solid-phase microextraction (SPME) gas chromatography–mass spectrometry (GC–MS) was used to analyse volatile flavour congeners. Hierarchical Multiple Factor Analysis was used to compare the product maps from samples taken at each whisky production stage and revealed a pattern of differences across the samples that could be tracked through the process. Although the flavour descriptors and volatile congeners composition changed at each stage, there were only marginal changes in the differentiation between samples, resulting in the same sample groups being found in all analyses. RV coefficients >0.90 for all analytical comparisons and >0.74 overall showed that all product maps were highly similar to each other and showed the same overall differentiation between samples. These results indicate that the analysis of fermented malt whisky wash may provide sufficient information to proceed to larger-scale industry trials, saving time and allowing a greater number of parameters to be explored. |
| first_indexed | 2024-03-11T02:45:58Z |
| format | Article |
| id | doaj.art-b043b76337bc4496b209a54fb39f65b8 |
| institution | Directory Open Access Journal |
| issn | 2306-5710 |
| language | English |
| last_indexed | 2024-03-11T02:45:58Z |
| publishDate | 2023-04-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Beverages |
| spelling | doaj.art-b043b76337bc4496b209a54fb39f65b82023-11-18T09:20:16ZengMDPI AGBeverages2306-57102023-04-01923710.3390/beverages9020037From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process SimulationsMartina Daute0Irene Baxter1Barry Harrison2Graeme Walker3Frances Jack4Division of Engineering and Food Sciences, Abertay University, Dundee DD1 1HG, UKThe Scotch Whisky Research Institute, Edinburgh EH14 4AH, UKThe Scotch Whisky Research Institute, Edinburgh EH14 4AH, UKDivision of Engineering and Food Sciences, Abertay University, Dundee DD1 1HG, UKThe Scotch Whisky Research Institute, Edinburgh EH14 4AH, UKNew product development for distilled spirits frequently involves experimental trials at the laboratory scale that attempt to replicate industrial-scale production processes. This process is time-consuming and limits the number of samples that can be analysed. The aim of the present study was to conduct laboratory-scale Scotch malt whisky production experiments to determine if samples taken from earlier in the production process, that is, directly after fermentation (wash stage) or after a single distillation (low wines stage), showed similar analytical differentiation compared to samples of fresh distillates (new make spirits). Napping, a rapid sensory method, was used to assess the impact on flavour characteristics while solid-phase microextraction (SPME) gas chromatography–mass spectrometry (GC–MS) was used to analyse volatile flavour congeners. Hierarchical Multiple Factor Analysis was used to compare the product maps from samples taken at each whisky production stage and revealed a pattern of differences across the samples that could be tracked through the process. Although the flavour descriptors and volatile congeners composition changed at each stage, there were only marginal changes in the differentiation between samples, resulting in the same sample groups being found in all analyses. RV coefficients >0.90 for all analytical comparisons and >0.74 overall showed that all product maps were highly similar to each other and showed the same overall differentiation between samples. These results indicate that the analysis of fermented malt whisky wash may provide sufficient information to proceed to larger-scale industry trials, saving time and allowing a greater number of parameters to be explored.https://www.mdpi.com/2306-5710/9/2/37whiskyflavour congenersfermentationyeastdistilled spiritNapping |
| spellingShingle | Martina Daute Irene Baxter Barry Harrison Graeme Walker Frances Jack From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process Simulations Beverages whisky flavour congeners fermentation yeast distilled spirit Napping |
| title | From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process Simulations |
| title_full | From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process Simulations |
| title_fullStr | From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process Simulations |
| title_full_unstemmed | From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process Simulations |
| title_short | From Fermented Wash to New Make Spirit: Assessing the Evolution of Flavour Characteristics of Scotch Whisky Using Lab-Scale Process Simulations |
| title_sort | from fermented wash to new make spirit assessing the evolution of flavour characteristics of scotch whisky using lab scale process simulations |
| topic | whisky flavour congeners fermentation yeast distilled spirit Napping |
| url | https://www.mdpi.com/2306-5710/9/2/37 |
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