Simple One–Pot Synthesis of Hexakis(2-alkoxy-1,5-phenyleneimine) Macrocycles by Precipitation–Driven Cyclization
Hexakis(2-alkoxy-1,5-phenyleneimine) macrocycles were synthesized using a simple one-pot procedure through precipitation-driven cyclization. The acetal-protected AB–type monomers, 2-alkoxy-5-aminobenzaldehyde diethyl acetals, underwent polycondensation in water or acid-containing tetrahydrofuran. Th...
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| Format: | Article |
| Language: | English |
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MDPI AG
2024-01-01
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| Series: | Macromol |
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| Online Access: | https://www.mdpi.com/2673-6209/4/1/1 |