Anion-exchange chromatography with post-column derivatization for the analysis of phytic acid in rice flour(柱后衍生离子色谱法分析米粉中植酸)
报道采用阴离子交换分离，0.1% FeCl3 and 2% HClO4在线柱后衍生，在290 nm波长检测，快速、方便地检测米粉中痕量植酸，该分离体系采用阴离子交换柱（Dionex IonPac AS7，250× 4 mm I. D.），以1.0 mL/min流速的0.25 mol/L HNO3为流动相，获得良好的分离效果而且具有较好的重现性，方法的测定范围为2~500 mg/L，检出限为0.56 mg/L，回收率为98.3% ~101.5%，结果令人满意....
| Main Authors: | , |
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| Format: | Article |
| Language: | zho |
| Published: |
Zhejiang University Press
2005-03-01
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| Series: | Zhejiang Daxue xuebao. Lixue ban |
| Subjects: | |
| Online Access: | https://doi.org/zjup/1008-9497.2005.32.2.201-203 |