1H-NMR as a Structural and Analytical Tool of Intra- and Intermolecular Hydrogen Bonds of Phenol-Containing Natural Products and Model Compounds

1H-NMR as a Structural and Analytical Tool of Intra- and Intermolecular Hydrogen Bonds of Phenol-Containing Natural Products and Model Compounds

Experimental parameters that influence the resolution of 1H-NMR phenol OH signals are critically evaluated with emphasis on the effects of pH, temperature and nature of the solvents. Extremely sharp peaks (Δν1/2 ≤ 2 Hz) can be obtained under optimized experimental conditions which allow the applicat...

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Bibliographic Details
Main Authors: Pantelis Charisiadis, Vassiliki G. Kontogianni, Constantinos G. Tsiafoulis, Andreas G. Tzakos, Michael Siskos, Ioannis P. Gerothanassis
Format: Article
Language:English
Published: MDPI AG 2014-09-01
Series:Molecules
Subjects:
chemical shifts
hydrogen bonding
1H-NMR
1H-13C HMBC
phenol OH
natural products
Online Access:http://www.mdpi.com/1420-3049/19/9/13643

Internet

http://www.mdpi.com/1420-3049/19/9/13643

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