Synthesis and comparative structural study of 2-(pyridin-2-yl)-1H-perimidine and its mono- and di-N-methylated analogues

Synthesis and comparative structural study of 2-(pyridin-2-yl)-1H-perimidine and its mono- and di-N-methylated analogues

The title compounds, 2-(pyridin-2-yl)-1H-perimidine (C16H11N3; 1), 1-methyl-2-(pyridin-2-yl)-1H-perimidine (C17H13N3; 2), and 1,3-dimethyl-2-(pyridin-2-yl)-1H-perimidinium iodide (C18H16N3+·I−; 3) were synthesized under mild conditions and their structures were determined by 1H NMR spectroscopy and...

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Bibliographic Details
Main Authors: Paulina Kalle, Sergei V. Tatarin, Alexander Yu. Zakharov, Marina A. Kiseleva, Stanislav I. Bezzubov
Format: Article
Language:English
Published: International Union of Crystallography 2021-02-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
perimidine
π–π stacking
hydrogen-bonding
nmr study
Online Access:http://scripts.iucr.org/cgi-bin/paper?S205698902100013X

Internet

http://scripts.iucr.org/cgi-bin/paper?S205698902100013X

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