In-situ evolution of anodic TiO2 nanotubes to ammonium oxofluorotitanate mesocrystals and their conversion to mesocrystalline TiO2

3D ordered superstructures of mesocrystalline NH4TiOF3 and (NH4)2TiOF4 are synthesized via in-situ evolution from anodic TiO2 nanotube arrays grown on the Ti metal substrate under high current density. As revealed by X-ray diffraction, scanning electron microscopy and transmission electron microscop...

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Bibliographic Details
Main Authors: Hui Li, Zixue Su
Format: Article
Language:English
Published: Elsevier 2021-12-01
Series:Electrochemistry Communications
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S1388248121002472