In-situ evolution of anodic TiO2 nanotubes to ammonium oxofluorotitanate mesocrystals and their conversion to mesocrystalline TiO2
3D ordered superstructures of mesocrystalline NH4TiOF3 and (NH4)2TiOF4 are synthesized via in-situ evolution from anodic TiO2 nanotube arrays grown on the Ti metal substrate under high current density. As revealed by X-ray diffraction, scanning electron microscopy and transmission electron microscop...
Main Authors: | , |
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Format: | Article |
Language: | English |
Published: |
Elsevier
2021-12-01
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Series: | Electrochemistry Communications |
Subjects: | |
Online Access: | http://www.sciencedirect.com/science/article/pii/S1388248121002472 |