Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and Characterization
Development of polypropylene (PP) films incorporating antioxidant-antimicrobial agents can inhibit microbial growth and reduce undesirable deteriorating reactions and can preserve the quality of food. This study was aimed to use a combination of sorbic acid (SA), butylated hydroxyanisole (BHA), and...
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MDPI AG
2021-03-01
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Online Access: | https://www.mdpi.com/2304-8158/10/4/722 |
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author | Seyed Hadi Peighambardoust Seyedeh Homa Fasihnia Seyed Jamaleddin Peighambardoust Mirian Pateiro Rubén Domínguez José M. Lorenzo |
author_facet | Seyed Hadi Peighambardoust Seyedeh Homa Fasihnia Seyed Jamaleddin Peighambardoust Mirian Pateiro Rubén Domínguez José M. Lorenzo |
author_sort | Seyed Hadi Peighambardoust |
collection | DOAJ |
description | Development of polypropylene (PP) films incorporating antioxidant-antimicrobial agents can inhibit microbial growth and reduce undesirable deteriorating reactions and can preserve the quality of food. This study was aimed to use a combination of sorbic acid (SA), butylated hydroxyanisole (BHA), and butylated hydroxytoluene (BHT) to provide a synergistic effect at their reduced concentrations. A Combination of the additives was more effective in enhancing mechanical properties compared to their single state in film composition. The PP-2%SA-3%BHA film (T<sub>3</sub>) had the highest tensile strength (17.9 MPa) and the lowest elongation at break (7.1%) than other films. The fourier-transform infrared (FTIR) proposed physical mixing of active additives within PP-matrix. Scanning electron microscopy showed uniform dispersion of the additives in PP-2%SA-1%BHT-1%BHA film (T<sub>4</sub>) compared to others. BHT containing films decreased the storage and loss moduli leading to weakening of film viscoelastic behaviour and reducing film melting point. The prepared active films showed higher antioxidant activity than control PP-film following an order of T<sub>4</sub> > T<sub>2</sub> > T<sub>3</sub> corresponding to DPPH radical scavenging values of 89.1, 83.4 and 79.1%, respectively. All active films inhibited gram-negative and gram-positive bacteria growth. The results of this study indicated that the prepared active films possess desirable mechanical, thermal, antioxidant and antimicrobial properties enabling their use in food packaging. |
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issn | 2304-8158 |
language | English |
last_indexed | 2024-03-10T12:48:39Z |
publishDate | 2021-03-01 |
publisher | MDPI AG |
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series | Foods |
spelling | doaj.art-bc5468b82d464ec198d4b4c6112698a92023-11-21T13:18:04ZengMDPI AGFoods2304-81582021-03-0110472210.3390/foods10040722Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and CharacterizationSeyed Hadi Peighambardoust0Seyedeh Homa Fasihnia1Seyed Jamaleddin Peighambardoust2Mirian Pateiro3Rubén Domínguez4José M. Lorenzo5Department of Food Science, College of Agriculture, University of Tabriz, Tabriz 5166616471, IranDepartment of Food Science, College of Agriculture, University of Tabriz, Tabriz 5166616471, IranFaculty of Chemical and Petroleum Engineering, University of Tabriz, Tabriz 5166616471, IranCentro Tecnológico de la Carne de Galicia, Rúa Galicia N° 4, Parque Tecnológico de Galicia, San Cibrao das Viñas, 32900 Ourense, SpainCentro Tecnológico de la Carne de Galicia, Rúa Galicia N° 4, Parque Tecnológico de Galicia, San Cibrao das Viñas, 32900 Ourense, SpainCentro Tecnológico de la Carne de Galicia, Rúa Galicia N° 4, Parque Tecnológico de Galicia, San Cibrao das Viñas, 32900 Ourense, SpainDevelopment of polypropylene (PP) films incorporating antioxidant-antimicrobial agents can inhibit microbial growth and reduce undesirable deteriorating reactions and can preserve the quality of food. This study was aimed to use a combination of sorbic acid (SA), butylated hydroxyanisole (BHA), and butylated hydroxytoluene (BHT) to provide a synergistic effect at their reduced concentrations. A Combination of the additives was more effective in enhancing mechanical properties compared to their single state in film composition. The PP-2%SA-3%BHA film (T<sub>3</sub>) had the highest tensile strength (17.9 MPa) and the lowest elongation at break (7.1%) than other films. The fourier-transform infrared (FTIR) proposed physical mixing of active additives within PP-matrix. Scanning electron microscopy showed uniform dispersion of the additives in PP-2%SA-1%BHT-1%BHA film (T<sub>4</sub>) compared to others. BHT containing films decreased the storage and loss moduli leading to weakening of film viscoelastic behaviour and reducing film melting point. The prepared active films showed higher antioxidant activity than control PP-film following an order of T<sub>4</sub> > T<sub>2</sub> > T<sub>3</sub> corresponding to DPPH radical scavenging values of 89.1, 83.4 and 79.1%, respectively. All active films inhibited gram-negative and gram-positive bacteria growth. The results of this study indicated that the prepared active films possess desirable mechanical, thermal, antioxidant and antimicrobial properties enabling their use in food packaging.https://www.mdpi.com/2304-8158/10/4/722active packagingpolypropyleneBHABHTsorbic acidmechanical properties |
spellingShingle | Seyed Hadi Peighambardoust Seyedeh Homa Fasihnia Seyed Jamaleddin Peighambardoust Mirian Pateiro Rubén Domínguez José M. Lorenzo Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and Characterization Foods active packaging polypropylene BHA BHT sorbic acid mechanical properties |
title | Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and Characterization |
title_full | Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and Characterization |
title_fullStr | Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and Characterization |
title_full_unstemmed | Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and Characterization |
title_short | Active Polypropylene-Based Films Incorporating Combined Antioxidants and Antimicrobials: Preparation and Characterization |
title_sort | active polypropylene based films incorporating combined antioxidants and antimicrobials preparation and characterization |
topic | active packaging polypropylene BHA BHT sorbic acid mechanical properties |
url | https://www.mdpi.com/2304-8158/10/4/722 |
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