Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocol

Abstract High-quality data are vital to the research field of paleointensity, which has long suffered from poor-quality and/or sparse data. Previous paleointensity work has established that repeatedly heating specimens increases the opportunity for thermochemical alteration to decrease the reliabili...

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Main Authors: J. Michael Grappone, James M. Russell, Andrew J. Biggin
Format: Article
Language:English
Published: SpringerOpen 2021-12-01
Series:Earth, Planets and Space
Subjects:
Online Access:https://doi.org/10.1186/s40623-021-01558-2
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author J. Michael Grappone
James M. Russell
Andrew J. Biggin
author_facet J. Michael Grappone
James M. Russell
Andrew J. Biggin
author_sort J. Michael Grappone
collection DOAJ
description Abstract High-quality data are vital to the research field of paleointensity, which has long suffered from poor-quality and/or sparse data. Previous paleointensity work has established that repeatedly heating specimens increases the opportunity for thermochemical alteration to decrease the reliability of paleointensity data. In addition, recent work has shown that repeatedly heating specimens in paleointensity experiments can also exaggerate the effects of non-ideal, non-single domain grains. Arai plots resulting from paleointensity experiments containing such grains are often curvilinear (two-slope) across most of the specimen’s unblocking temperature spectrum, except in the temperature range nearest to the grains’ Curie temperature. This study tests the following strategy to mitigate these effects: that of performing a Thellier paleointensity experiment using fewer temperature steps that are also concentrated at higher temperatures. For this purpose, we use natural specimens with well-constrained rock magnetic data from the Hawaiian Scientific Observation Hole 1 (SOH1) drill core in paleointensity experiments with starting temperatures ranging from 200 °C to 500+ °C. Those experiments that focused in on the portion of the unblocking temperature spectrum nearest the Curie temperature of the specimen (HiTeCT) had an exceptionally low success rate, whereas those with initial temperatures at comparatively moderate temperatures (200–400 °C) had high success rates (~ 70%). Thermochemical alteration was minimized with a start temperature of 400 °C, but the curvature of the Arai plots had no clear dependance on start temperature. We conclude herein that increasing the start temperature can help avoid the effects of low-temperature alterations. Additionally, we found that the approach of focusing in on the highest temperature range is not a feasible one to apply in paleointensity experiments, in general, and consider this likely to be a result of a lack of intermediate-temperature checks for alteration and insufficient independence of temperature steps. Graphical abstract
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spelling doaj.art-bc9b33f08812408c9bc1f5f0fecdaa002022-12-21T18:45:10ZengSpringerOpenEarth, Planets and Space1880-59812021-12-0173111010.1186/s40623-021-01558-2Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocolJ. Michael Grappone0James M. Russell1Andrew J. Biggin2Geomagnetism Laboratory, School of Environmental Sciences, University of LiverpoolGeomagnetism Laboratory, School of Environmental Sciences, University of LiverpoolGeomagnetism Laboratory, School of Environmental Sciences, University of LiverpoolAbstract High-quality data are vital to the research field of paleointensity, which has long suffered from poor-quality and/or sparse data. Previous paleointensity work has established that repeatedly heating specimens increases the opportunity for thermochemical alteration to decrease the reliability of paleointensity data. In addition, recent work has shown that repeatedly heating specimens in paleointensity experiments can also exaggerate the effects of non-ideal, non-single domain grains. Arai plots resulting from paleointensity experiments containing such grains are often curvilinear (two-slope) across most of the specimen’s unblocking temperature spectrum, except in the temperature range nearest to the grains’ Curie temperature. This study tests the following strategy to mitigate these effects: that of performing a Thellier paleointensity experiment using fewer temperature steps that are also concentrated at higher temperatures. For this purpose, we use natural specimens with well-constrained rock magnetic data from the Hawaiian Scientific Observation Hole 1 (SOH1) drill core in paleointensity experiments with starting temperatures ranging from 200 °C to 500+ °C. Those experiments that focused in on the portion of the unblocking temperature spectrum nearest the Curie temperature of the specimen (HiTeCT) had an exceptionally low success rate, whereas those with initial temperatures at comparatively moderate temperatures (200–400 °C) had high success rates (~ 70%). Thermochemical alteration was minimized with a start temperature of 400 °C, but the curvature of the Arai plots had no clear dependance on start temperature. We conclude herein that increasing the start temperature can help avoid the effects of low-temperature alterations. Additionally, we found that the approach of focusing in on the highest temperature range is not a feasible one to apply in paleointensity experiments, in general, and consider this likely to be a result of a lack of intermediate-temperature checks for alteration and insufficient independence of temperature steps. Graphical abstracthttps://doi.org/10.1186/s40623-021-01558-2PaleomagnetismPaleointensityMethodologyRock magnetism
spellingShingle J. Michael Grappone
James M. Russell
Andrew J. Biggin
Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocol
Earth, Planets and Space
Paleomagnetism
Paleointensity
Methodology
Rock magnetism
title Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocol
title_full Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocol
title_fullStr Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocol
title_full_unstemmed Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocol
title_short Investigating the utility of a high-temperature Thellier-style paleointensity experimental protocol
title_sort investigating the utility of a high temperature thellier style paleointensity experimental protocol
topic Paleomagnetism
Paleointensity
Methodology
Rock magnetism
url https://doi.org/10.1186/s40623-021-01558-2
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