Argon irradiation effects on the structural and optical properties of reactively sputtered CrN films

The present study deals with CrN films irradiated at room temperature (RT) with 200 keV Ar+ ions. The CrN layers were deposited by d.c. reactive sputtering on Si (100) wafers, at nitrogen partial pressure of 5×10-4 mbar, to a total thickness of 280 nm. The substrates were held at 150ºC duri...

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Main Authors: Novaković M., Popović M., Bibić N.
Format: Article
Language:English
Published: International Institute for the Science of Sintering, Beograd 2015-01-01
Series:Science of Sintering
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/0350-820X/2015/0350-820X1502187N.pdf
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author Novaković M.
Popović M.
Bibić N.
author_facet Novaković M.
Popović M.
Bibić N.
author_sort Novaković M.
collection DOAJ
description The present study deals with CrN films irradiated at room temperature (RT) with 200 keV Ar+ ions. The CrN layers were deposited by d.c. reactive sputtering on Si (100) wafers, at nitrogen partial pressure of 5×10-4 mbar, to a total thickness of 280 nm. The substrates were held at 150ºC during deposition. After deposition the CrN layers were irradiated with 200 keV Ar+ ions to the fluences of 5×1015 - 2×1016 ions/cm2. Structural characterization was performed with Rutherford backscattering spectroscopy (RBS), cross-sectional transmission electron microscopy (XTEM) and X-ray diffraction (XRD). Spectroscopic ellipsometry measurements were carried out in order to study optical properties of the samples. The irradiations caused the microstructrual changes in CrN layers, but no amorphization even at the highest argon fluence of 2×1016 ions/cm2. Observed changes in microstructure were correlated with the variation in optical parameters. It was found that both refractive index and extinction coefficient are strongly dependent on the defect concentration in CrN layers. [Projekat Ministarstva nauke Republike Srbije, br. III 45005]
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spelling doaj.art-cf7f4d2897864f2ca2cfcd3c0779f33b2022-12-21T18:39:13ZengInternational Institute for the Science of Sintering, BeogradScience of Sintering0350-820X1820-74132015-01-0147218719410.2298/SOS1502187N0350-820X1502187NArgon irradiation effects on the structural and optical properties of reactively sputtered CrN filmsNovaković M.0Popović M.1Bibić N.2VINČA Institute of Nuclear Sciences, BelgradeVINČA Institute of Nuclear Sciences, BelgradeVINČA Institute of Nuclear Sciences, BelgradeThe present study deals with CrN films irradiated at room temperature (RT) with 200 keV Ar+ ions. The CrN layers were deposited by d.c. reactive sputtering on Si (100) wafers, at nitrogen partial pressure of 5×10-4 mbar, to a total thickness of 280 nm. The substrates were held at 150ºC during deposition. After deposition the CrN layers were irradiated with 200 keV Ar+ ions to the fluences of 5×1015 - 2×1016 ions/cm2. Structural characterization was performed with Rutherford backscattering spectroscopy (RBS), cross-sectional transmission electron microscopy (XTEM) and X-ray diffraction (XRD). Spectroscopic ellipsometry measurements were carried out in order to study optical properties of the samples. The irradiations caused the microstructrual changes in CrN layers, but no amorphization even at the highest argon fluence of 2×1016 ions/cm2. Observed changes in microstructure were correlated with the variation in optical parameters. It was found that both refractive index and extinction coefficient are strongly dependent on the defect concentration in CrN layers. [Projekat Ministarstva nauke Republike Srbije, br. III 45005]http://www.doiserbia.nb.rs/img/doi/0350-820X/2015/0350-820X1502187N.pdfCrN filmsion irradiationTEMRBSXRDellipsometry
spellingShingle Novaković M.
Popović M.
Bibić N.
Argon irradiation effects on the structural and optical properties of reactively sputtered CrN films
Science of Sintering
CrN films
ion irradiation
TEM
RBS
XRD
ellipsometry
title Argon irradiation effects on the structural and optical properties of reactively sputtered CrN films
title_full Argon irradiation effects on the structural and optical properties of reactively sputtered CrN films
title_fullStr Argon irradiation effects on the structural and optical properties of reactively sputtered CrN films
title_full_unstemmed Argon irradiation effects on the structural and optical properties of reactively sputtered CrN films
title_short Argon irradiation effects on the structural and optical properties of reactively sputtered CrN films
title_sort argon irradiation effects on the structural and optical properties of reactively sputtered crn films
topic CrN films
ion irradiation
TEM
RBS
XRD
ellipsometry
url http://www.doiserbia.nb.rs/img/doi/0350-820X/2015/0350-820X1502187N.pdf
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AT popovicm argonirradiationeffectsonthestructuralandopticalpropertiesofreactivelysputteredcrnfilms
AT bibicn argonirradiationeffectsonthestructuralandopticalpropertiesofreactivelysputteredcrnfilms