Online In-Tube Solid-Phase Microextraction Coupled with Liquid Chromatography–Tandem Mass Spectrometry for Automated Analysis of Four Sulfated Steroid Metabolites in Saliva Samples

Online In-Tube Solid-Phase Microextraction Coupled with Liquid Chromatography–Tandem Mass Spectrometry for Automated Analysis of Four Sulfated Steroid Metabolites in Saliva Samples

Accurate measurement of sulfated steroid metabolite concentrations can not only enable the elucidation of the mechanisms regulating steroid metabolism, but also lead to the diagnosis of various related diseases. The present study describes a simple and sensitive method for the simultaneous determina...

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Bibliographic Details
Main Authors: Hiroyuki Kataoka, Daiki Nakayama
Format: Article
Language:English
Published: MDPI AG 2022-05-01
Series:Molecules
Subjects:
sulfated steroid metabolites
saliva
online automated analysis
in-tube solid-phase microextraction (IT-SPME)
liquid chromatography–tandem mass spectrometry (LC–MS/MS)
stable isotope dilution
Online Access:https://www.mdpi.com/1420-3049/27/10/3225

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https://www.mdpi.com/1420-3049/27/10/3225

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