Limits of Resolution and Sensitivity of Proton Detected MAS Solid-State NMR Experiments at 111 kHz in Deuterated and Protonated Proteins

Limits of Resolution and Sensitivity of Proton Detected MAS Solid-State NMR Experiments at 111 kHz in Deuterated and Protonated Proteins

Abstract MAS solid-state NMR is capable of determining structures of protonated solid proteins using proton-detected experiments. These experiments are performed at MAS rotation frequency of around 110 kHz, employing 0.5 mg of material. Here, we compare 1H, 13C correlation spectra obtained from prot...

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Bibliographic Details
Main Authors: Kai Xue, Riddhiman Sarkar, Carina Motz, Sam Asami, Diana C. Rodriguez Camargo, Venita Decker, Sebastian Wegner, Zdenek Tosner, Bernd Reif
Format: Article
Language:English
Published: Nature Portfolio 2017-08-01
Series:Scientific Reports
Online Access:https://doi.org/10.1038/s41598-017-07253-1

Internet

https://doi.org/10.1038/s41598-017-07253-1

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