Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds
The present work include preparation of three ligands (Schiff base) by condensation of (Phthaldialdehyde) with 1,3-diamino-2-propanol) to give ligands (L) L: (1Z,6Z)-4,5-dihydro -3H-2,6-benzodiazonin-4-ol o characterize the structure of prepared ligands and their complexes, elemental analysis (C.H...
| Hoofdauteur: | |
|---|---|
| Formaat: | Artikel |
| Taal: | English |
| Gepubliceerd in: |
University of Thi-Qar
2019-05-01
|
| Reeks: | مجلة علوم ذي قار |
| Onderwerpen: | |
| Online toegang: | https://mail.jsci.utq.edu.iq/index.php/main/article/view/119 |
| _version_ | 1827635946355425280 |
|---|---|
| author | Fatima F. Hassan |
| author_facet | Fatima F. Hassan |
| author_sort | Fatima F. Hassan |
| collection | DOAJ |
| description |
The present work include preparation of three ligands (Schiff base) by condensation of (Phthaldialdehyde) with
1,3-diamino-2-propanol) to give ligands (L)
L: (1Z,6Z)-4,5-dihydro -3H-2,6-benzodiazonin-4-ol
o characterize the structure of prepared ligands and their complexes, elemental analysis (C.H.N),Infrared
Spectroscopy (IR), Nuclear Magnetic Resonance Spectroscopy(
1
H-NMR),Mass Spectra and Molar conductivity
echniques were applied . The results showed that:
- The complexes of [Co(III) and Cr(III)] for ligand have shown octahedral configuration.
- Complexes of [ Ni(II)] with ligands have shown tetrahedral configuration.
|
| first_indexed | 2024-03-09T15:34:26Z |
| format | Article |
| id | doaj.art-d259028ac69f4df4a6c8cfd19b9f9c0f |
| institution | Directory Open Access Journal |
| issn | 1991-8690 2709-0256 |
| language | English |
| last_indexed | 2024-03-09T15:34:26Z |
| publishDate | 2019-05-01 |
| publisher | University of Thi-Qar |
| record_format | Article |
| series | مجلة علوم ذي قار |
| spelling | doaj.art-d259028ac69f4df4a6c8cfd19b9f9c0f2023-11-26T09:41:26ZengUniversity of Thi-Qarمجلة علوم ذي قار1991-86902709-02562019-05-0152Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds Fatima F. Hassan The present work include preparation of three ligands (Schiff base) by condensation of (Phthaldialdehyde) with 1,3-diamino-2-propanol) to give ligands (L) L: (1Z,6Z)-4,5-dihydro -3H-2,6-benzodiazonin-4-ol o characterize the structure of prepared ligands and their complexes, elemental analysis (C.H.N),Infrared Spectroscopy (IR), Nuclear Magnetic Resonance Spectroscopy( 1 H-NMR),Mass Spectra and Molar conductivity echniques were applied . The results showed that: - The complexes of [Co(III) and Cr(III)] for ligand have shown octahedral configuration. - Complexes of [ Ni(II)] with ligands have shown tetrahedral configuration. https://mail.jsci.utq.edu.iq/index.php/main/article/view/119Schiff base complexes |
| spellingShingle | Fatima F. Hassan Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds مجلة علوم ذي قار Schiff base complexes |
| title | Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds |
| title_full | Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds |
| title_fullStr | Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds |
| title_full_unstemmed | Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds |
| title_short | Synthesis, Spectroscopic Studies of Some Transition Metal Complexes of Schiff Bases Derived from Diamine Compounds |
| title_sort | synthesis spectroscopic studies of some transition metal complexes of schiff bases derived from diamine compounds |
| topic | Schiff base complexes |
| url | https://mail.jsci.utq.edu.iq/index.php/main/article/view/119 |
| work_keys_str_mv | AT fatimafhassan synthesisspectroscopicstudiesofsometransitionmetalcomplexesofschiffbasesderivedfromdiaminecompounds |