Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan Region

This study was conducted with the aim of developing fruit spirits by utilizing old (autochthonous) apple and pear cultivars that can be attractive to both consumers and producers. Consumers of spirits could enjoy the unique flavor, and producers could gain an opportunity for brand development. In to...

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Main Authors: Nermina Spaho, Fuad Gaši, Erich Leitner, Milenko Blesić, Asima Akagić, Sanja Oručević Žuljević, Mirsad Kurtović, Davorka Đukić Ratković, Mirela Smajić Murtić, Milica Fotirić Akšić, Mekjell Meland
Format: Article
Language:English
Published: MDPI AG 2021-06-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/10/6/1258
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author Nermina Spaho
Fuad Gaši
Erich Leitner
Milenko Blesić
Asima Akagić
Sanja Oručević Žuljević
Mirsad Kurtović
Davorka Đukić Ratković
Mirela Smajić Murtić
Milica Fotirić Akšić
Mekjell Meland
author_facet Nermina Spaho
Fuad Gaši
Erich Leitner
Milenko Blesić
Asima Akagić
Sanja Oručević Žuljević
Mirsad Kurtović
Davorka Đukić Ratković
Mirela Smajić Murtić
Milica Fotirić Akšić
Mekjell Meland
author_sort Nermina Spaho
collection DOAJ
description This study was conducted with the aim of developing fruit spirits by utilizing old (autochthonous) apple and pear cultivars that can be attractive to both consumers and producers. Consumers of spirits could enjoy the unique flavor, and producers could gain an opportunity for brand development. In total, eight old apple cultivars (Sarija, Žuja, Samoniklica, Prijedorska zelenika, Bobovec, Masnjača, Lijepocvjetka, and Šarenika) and three pear cultivars (Budaljača, Krakača, and Kalićanka) from Bosnia and Herzegovina were used for the spirits production and for characterizing the flavor of distillates. Golden Delicious was used as a representative of commercial apple cultivar. The aroma profile was conducted through the identification of minor volatile organic compounds (VOCs) and the sensory perception of spirits. Analysis of the VOCs was performed by gas chromatography mass spectroscopy (GC/MS) techniques after enrichment via solid-phase microextraction (SPME). Sensory evaluation was performed by 12 trained panelists. Overall, 35 minor volatile compounds were found in spirits: 13 esters, 7 alcohols, 6 acids, 5 terpenes, and 4 aldehydes. Significant differences were detected in the distribution and quantity of the VOCs, which were fruit cultivar-dependent. Spirits made from Šarenika apple cultivar showed the largest amount of all acids, especially short- and medium-chain fatty acids; however, this richness was not correlated with pleasant sensory attributes. Spirits obtained from Prijedorska zelenika and Masnjača apple cultivars had the best sensory attributes. Budeljača and Krakača pears are promising cultivars as flavoring in spirits production.
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spelling doaj.art-d401515b2c7548ef87dbe31c5eb6ef4e2023-11-21T22:24:55ZengMDPI AGFoods2304-81582021-06-01106125810.3390/foods10061258Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan RegionNermina Spaho0Fuad Gaši1Erich Leitner2Milenko Blesić3Asima Akagić4Sanja Oručević Žuljević5Mirsad Kurtović6Davorka Đukić Ratković7Mirela Smajić Murtić8Milica Fotirić Akšić9Mekjell Meland10Faculty of Agriculture and Food Sciences, University of Sarajevo, 71000 Sarajevo, Bosnia and HerzegovinaFaculty of Agriculture and Food Sciences, University of Sarajevo, 71000 Sarajevo, Bosnia and HerzegovinaInstitute of Analytical Chemistry and Food Chemistry (6450), Graz University of Technology, 8010 Graz, AustriaFaculty of Agriculture and Food Sciences, University of Sarajevo, 71000 Sarajevo, Bosnia and HerzegovinaFaculty of Agriculture and Food Sciences, University of Sarajevo, 71000 Sarajevo, Bosnia and HerzegovinaFaculty of Agriculture and Food Sciences, University of Sarajevo, 71000 Sarajevo, Bosnia and HerzegovinaFaculty of Agriculture and Food Sciences, University of Sarajevo, 71000 Sarajevo, Bosnia and HerzegovinaDisttllery BMB Delta, Jablanica, 173, 78405 Gradiška, Bosnia and HerzegovinaFaculty of Agriculture and Food Sciences, University of Sarajevo, 71000 Sarajevo, Bosnia and HerzegovinaFaculty of Agriculture, University of Belgrade, Nemanjina 6, 11080 Belgrade, SerbiaNorwegian Institute of Bioeconomy Research, NIBIO Ullensvang, Ullensvangvegen 1003, N-5781 Lofthus, NorwayThis study was conducted with the aim of developing fruit spirits by utilizing old (autochthonous) apple and pear cultivars that can be attractive to both consumers and producers. Consumers of spirits could enjoy the unique flavor, and producers could gain an opportunity for brand development. In total, eight old apple cultivars (Sarija, Žuja, Samoniklica, Prijedorska zelenika, Bobovec, Masnjača, Lijepocvjetka, and Šarenika) and three pear cultivars (Budaljača, Krakača, and Kalićanka) from Bosnia and Herzegovina were used for the spirits production and for characterizing the flavor of distillates. Golden Delicious was used as a representative of commercial apple cultivar. The aroma profile was conducted through the identification of minor volatile organic compounds (VOCs) and the sensory perception of spirits. Analysis of the VOCs was performed by gas chromatography mass spectroscopy (GC/MS) techniques after enrichment via solid-phase microextraction (SPME). Sensory evaluation was performed by 12 trained panelists. Overall, 35 minor volatile compounds were found in spirits: 13 esters, 7 alcohols, 6 acids, 5 terpenes, and 4 aldehydes. Significant differences were detected in the distribution and quantity of the VOCs, which were fruit cultivar-dependent. Spirits made from Šarenika apple cultivar showed the largest amount of all acids, especially short- and medium-chain fatty acids; however, this richness was not correlated with pleasant sensory attributes. Spirits obtained from Prijedorska zelenika and Masnjača apple cultivars had the best sensory attributes. Budeljača and Krakača pears are promising cultivars as flavoring in spirits production.https://www.mdpi.com/2304-8158/10/6/1258old applesold pearsfruit spiritsvolatile aroma compounds
spellingShingle Nermina Spaho
Fuad Gaši
Erich Leitner
Milenko Blesić
Asima Akagić
Sanja Oručević Žuljević
Mirsad Kurtović
Davorka Đukić Ratković
Mirela Smajić Murtić
Milica Fotirić Akšić
Mekjell Meland
Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan Region
Foods
old apples
old pears
fruit spirits
volatile aroma compounds
title Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan Region
title_full Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan Region
title_fullStr Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan Region
title_full_unstemmed Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan Region
title_short Characterization of Volatile Compounds and Flavor in Spirits of Old Apple and Pear Cultivars from the Balkan Region
title_sort characterization of volatile compounds and flavor in spirits of old apple and pear cultivars from the balkan region
topic old apples
old pears
fruit spirits
volatile aroma compounds
url https://www.mdpi.com/2304-8158/10/6/1258
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