Electrochemical Synthesis of 3,5-Bis(acyl)-1,2,4-thiadiazoles through n-Bu4NI-mediated Oxidative Dimerization of α-Oxothioamides

Electrochemical Synthesis of 3,5-Bis(acyl)-1,2,4-thiadiazoles through n-Bu4NI-mediated Oxidative Dimerization of α-Oxothioamides

An electrochemical synthesis of 3,5-bis(acyl)-1,2,4-thiadiazoles by the oxidative dimerization of α-oxothioamides with assistance of tetra-n-butylammonium iodide (TBAI) as electrolyte and mediator under constant current electrolysis (CCE) is reported. Herein, this approach is an example for S–N bond...

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Bibliographic Details
Main Authors: Mahadev SHIVARAJ, Rajaghatta N SURESH, Toreshettahally R SWAROOP, Manikyanahally N KUMARA, Kanchugarakoppal S RANGAPPA, Kempegowda MANTELINGU, Adaganahalli Boregowda MAMATHA DEVI, Madihalli Prasanna MANASA, Muddegowda UMASHANKARA
Format: Article
Language:English
Published: The Electrochemical Society of Japan 2023-12-01
Series:Electrochemistry
Subjects:
electrochemical synthesis
α-oxodithioesters
α-oxothioamides
1,2,4-thiadiazoles
Online Access:https://www.jstage.jst.go.jp/article/electrochemistry/91/12/91_23-67131/_html/-char/en

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https://www.jstage.jst.go.jp/article/electrochemistry/91/12/91_23-67131/_html/-char/en

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