Synthesis, crystal structure and Hirshfeld surface analysis of tert-butyl N-acetylcarbamate

Synthesis, crystal structure and Hirshfeld surface analysis of tert-butyl N-acetylcarbamate

This article reports a practical synthesis of tert-butyl acetylcarbamate, C7H13NO3, from N-Boc-thioacetamide and the study of its crystal structure. The reaction proceeds in the presence of natural phosphate as a catalyst, with excellent yield, simple workup and benign environment. The crystal struc...

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Bibliographic Details
Main Authors: Aly Dawa El Mestehdi, Moctar Abba, Mohamed Lemine El Housseine, Abderrahmane Ould Hadou, Aliou Hamady Barry, Brahim Ould Elemine, Christian Jelsch, Mohamed Gaye
Format: Article
Language:English
Published: International Union of Crystallography 2022-10-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
x-ray crystal structure
tert-butyl acetylcarbamate
natural phosphate
mauritanian phosphate deposit
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989022009483

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http://scripts.iucr.org/cgi-bin/paper?S2056989022009483

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