Synthesis of potassium–sodium niobate (KNN) from NbO2

KxNa1-xNbO3 (0 < x < 1) were synthesized via hydrothermal method using niobium dioxide (NbO2) as the niobium source instead of the most common one, Nb2O5. Potassium-rich KxNa1-xNbO3 (x > 0.5) was obtained from 8 M total hydroxide concentration after 6 h of reaction at 200 °C. Rietveld refin...

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Bibliographic Details
Main Authors: Cerem Piskin, Levent Karacasulu, Mauro Bortolotti, Cekdar Vakifahmetoglu
Format: Article
Language:English
Published: Elsevier 2021-09-01
Series:Open Ceramics
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S266653952100105X