Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film

The food wastes have significant amount of functional ingredients that have valorization potential. Citrus limon (lemon), Mangifera Indica (mango) peels are maximally used as waste in food industries in all over the worlds. This work aimed to extract pectin from mango and pectin peels at different c...

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Main Authors: Rezaul Karim, Kamrun Nahar, Fatema Tuz Zohora, Md. Monarul Islam, Riyadh Hossen Bhuiyan, M Sarwar Jahan, Md. Aftab Ali Shaikh
Format: Article
Language:English
Published: Elsevier 2022-12-01
Series:Carbohydrate Polymer Technologies and Applications
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2666893922000731
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author Rezaul Karim
Kamrun Nahar
Fatema Tuz Zohora
Md. Monarul Islam
Riyadh Hossen Bhuiyan
M Sarwar Jahan
Md. Aftab Ali Shaikh
author_facet Rezaul Karim
Kamrun Nahar
Fatema Tuz Zohora
Md. Monarul Islam
Riyadh Hossen Bhuiyan
M Sarwar Jahan
Md. Aftab Ali Shaikh
author_sort Rezaul Karim
collection DOAJ
description The food wastes have significant amount of functional ingredients that have valorization potential. Citrus limon (lemon), Mangifera Indica (mango) peels are maximally used as waste in food industries in all over the worlds. This work aimed to extract pectin from mango and pectin peels at different conditions, and pectin yield, degree of esterification (DE), intrinsic viscosity (η) and molecular weight (Mw) were determined. The best conditions of extraction were pH 2, temperature 80 °C, time 4 h for lemon and 5 h for mango, where pectin yields were 30.60 ± 0.95 and 31.70 ± 1.04%, respectively. At this condition, DE, η, Mw were 42.02%, 0.177 and 42,316 g/mol for lemon peel while 30.60%, 0.05 and 8364.01 g/mol for mango peel, respectively. The extracted pectin under optimal conditions was used to fabricate pectin-silica based film. All the composition of films showed considerable mechanical properties due to the presence of silica. The highest values of tensile strength and young modulus were found 61.31 MPa and 16.49 MPa, respectively, at the silica percentage of 1.25% (w/v) where toughness and elongation at break were decreased due to the more bonding between pectin and silica. This study demonstrated that incorporating silica at 1.25% (w/v) can improve the physicochemical properties of pectin film.
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spelling doaj.art-ea5c49a656cf451382b70ec0a5be77772022-12-22T04:18:29ZengElsevierCarbohydrate Polymer Technologies and Applications2666-89392022-12-014100258Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable filmRezaul Karim0Kamrun Nahar1Fatema Tuz Zohora2Md. Monarul Islam3Riyadh Hossen Bhuiyan4M Sarwar Jahan5Md. Aftab Ali Shaikh6BCSIR Laboratories Dhaka, Bangladesh Council of Scientific and Industrial Research (BCSIR), 1205, Dhanmondi, Dhaka, BangladeshBCSIR Laboratories Dhaka, Bangladesh Council of Scientific and Industrial Research (BCSIR), 1205, Dhanmondi, Dhaka, BangladeshBCSIR Laboratories Dhaka, Bangladesh Council of Scientific and Industrial Research (BCSIR), 1205, Dhanmondi, Dhaka, BangladeshBCSIR Laboratories Dhaka, Bangladesh Council of Scientific and Industrial Research (BCSIR), 1205, Dhanmondi, Dhaka, BangladeshBCSIR Laboratories Dhaka, Bangladesh Council of Scientific and Industrial Research (BCSIR), 1205, Dhanmondi, Dhaka, BangladeshBCSIR Laboratories Dhaka, Bangladesh Council of Scientific and Industrial Research (BCSIR), 1205, Dhanmondi, Dhaka, Bangladesh; Corresponding author.Bangladesh Council of Scientific and Industrial Research (BCSIR), 1205, Dhanmondi, Dhaka, Bangladesh; Department of Chemistry, University of Dhaka, 1000, Dhaka, BangladeshThe food wastes have significant amount of functional ingredients that have valorization potential. Citrus limon (lemon), Mangifera Indica (mango) peels are maximally used as waste in food industries in all over the worlds. This work aimed to extract pectin from mango and pectin peels at different conditions, and pectin yield, degree of esterification (DE), intrinsic viscosity (η) and molecular weight (Mw) were determined. The best conditions of extraction were pH 2, temperature 80 °C, time 4 h for lemon and 5 h for mango, where pectin yields were 30.60 ± 0.95 and 31.70 ± 1.04%, respectively. At this condition, DE, η, Mw were 42.02%, 0.177 and 42,316 g/mol for lemon peel while 30.60%, 0.05 and 8364.01 g/mol for mango peel, respectively. The extracted pectin under optimal conditions was used to fabricate pectin-silica based film. All the composition of films showed considerable mechanical properties due to the presence of silica. The highest values of tensile strength and young modulus were found 61.31 MPa and 16.49 MPa, respectively, at the silica percentage of 1.25% (w/v) where toughness and elongation at break were decreased due to the more bonding between pectin and silica. This study demonstrated that incorporating silica at 1.25% (w/v) can improve the physicochemical properties of pectin film.http://www.sciencedirect.com/science/article/pii/S2666893922000731Lemon peelMango peelPectin yield optimizationDegree of esterificationIntrinsic viscosityBiodegradable packaging film
spellingShingle Rezaul Karim
Kamrun Nahar
Fatema Tuz Zohora
Md. Monarul Islam
Riyadh Hossen Bhuiyan
M Sarwar Jahan
Md. Aftab Ali Shaikh
Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film
Carbohydrate Polymer Technologies and Applications
Lemon peel
Mango peel
Pectin yield optimization
Degree of esterification
Intrinsic viscosity
Biodegradable packaging film
title Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film
title_full Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film
title_fullStr Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film
title_full_unstemmed Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film
title_short Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film
title_sort pectin from lemon and mango peel extraction characterisation and application in biodegradable film
topic Lemon peel
Mango peel
Pectin yield optimization
Degree of esterification
Intrinsic viscosity
Biodegradable packaging film
url http://www.sciencedirect.com/science/article/pii/S2666893922000731
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