Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in Chengdu

To investigate the pesticide residues in fruits and vegetables and their dietary risk to Chengdu residents. A total of 203 samples of 9 kinds of fruits and vegetables were collected from large farmer markets and supermarkets in Chengdu. The modified GB 23200.113-2018 QuEChERS pre-treatment method co...

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Main Authors: Wei CHANG, Hui LI, Chunmei LI, Qiang HE, Zhan HUANG, Jiangtao CHEN, Pengyan LV, Meijie SONG, Qingsong LI, Hong LIU, Ao LI
Format: Article
Language:zho
Published: The editorial department of Science and Technology of Food Industry 2022-03-01
Series:Shipin gongye ke-ji
Subjects:
Online Access:http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021060041
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author Wei CHANG
Hui LI
Chunmei LI
Qiang HE
Zhan HUANG
Jiangtao CHEN
Pengyan LV
Meijie SONG
Qingsong LI
Hong LIU
Ao LI
author_facet Wei CHANG
Hui LI
Chunmei LI
Qiang HE
Zhan HUANG
Jiangtao CHEN
Pengyan LV
Meijie SONG
Qingsong LI
Hong LIU
Ao LI
author_sort Wei CHANG
collection DOAJ
description To investigate the pesticide residues in fruits and vegetables and their dietary risk to Chengdu residents. A total of 203 samples of 9 kinds of fruits and vegetables were collected from large farmer markets and supermarkets in Chengdu. The modified GB 23200.113-2018 QuEChERS pre-treatment method combined with gas chromatography-triple quadrupole-tandem mass spectrometry method was used to analyze 48 pesticides. Chronic dietary intake risk was assessed by a combination of fruit and vegetable consumption of residents in big cities and the food safety index method. It showed good linear relationships for 48 pesticides in the range of 0.025~25 μg/kg, with the correlation coefficients higher than 0.99. The average recoveries of the pesticides were 60.1%~117.7%, with relative standard deviations less than 10%. The limits of quantification were 0.083~3.3 μg/kg. This method could meet the requirements for trace determination of the 48 pesticides in fruits and vegetables. The detection rate of pesticide residues in 203 fruit and vegetable samples was 50.2%. Six pesticides were detected in all the samples, and all of them did not exceed the maximum residue limits. The detection rate of pyraclostrobin was the highest, being 29.1%. Various kinds of fruits and vegetables were polluted differently by pesticides. Berries and other small kinds of fruits, represented by strawberries, had the highest detection rate up to 91.7%. The results of chronic dietary exposure assessment showed that the food safety index values of all detected pesticides ranged from 0.00002 to 0.004, much less than 1. But the daily intake of propargite was relatively high (0.00257 mg/d), which should be paid more attention in the future.
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spelling doaj.art-fff76770096a4d609e923e31166c26912022-12-22T04:39:09ZzhoThe editorial department of Science and Technology of Food IndustryShipin gongye ke-ji1002-03062022-03-0143625826810.13386/j.issn1002-0306.20210600412021060041-6Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in ChengduWei CHANG0Hui LI1Chunmei LI2Qiang HE3Zhan HUANG4Jiangtao CHEN5Pengyan LV6Meijie SONG7Qingsong LI8Hong LIU9Ao LI10Sichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaInstitute of Food Science and Technology, Chinese Academy of Agricultural Science, Beijing 100193, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaSichuang Light Industry Research and Design Institute Co., Ltd., Chengdu 610081, ChinaTo investigate the pesticide residues in fruits and vegetables and their dietary risk to Chengdu residents. A total of 203 samples of 9 kinds of fruits and vegetables were collected from large farmer markets and supermarkets in Chengdu. The modified GB 23200.113-2018 QuEChERS pre-treatment method combined with gas chromatography-triple quadrupole-tandem mass spectrometry method was used to analyze 48 pesticides. Chronic dietary intake risk was assessed by a combination of fruit and vegetable consumption of residents in big cities and the food safety index method. It showed good linear relationships for 48 pesticides in the range of 0.025~25 μg/kg, with the correlation coefficients higher than 0.99. The average recoveries of the pesticides were 60.1%~117.7%, with relative standard deviations less than 10%. The limits of quantification were 0.083~3.3 μg/kg. This method could meet the requirements for trace determination of the 48 pesticides in fruits and vegetables. The detection rate of pesticide residues in 203 fruit and vegetable samples was 50.2%. Six pesticides were detected in all the samples, and all of them did not exceed the maximum residue limits. The detection rate of pyraclostrobin was the highest, being 29.1%. Various kinds of fruits and vegetables were polluted differently by pesticides. Berries and other small kinds of fruits, represented by strawberries, had the highest detection rate up to 91.7%. The results of chronic dietary exposure assessment showed that the food safety index values of all detected pesticides ranged from 0.00002 to 0.004, much less than 1. But the daily intake of propargite was relatively high (0.00257 mg/d), which should be paid more attention in the future.http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021060041quechersgas chromatography-triple quadrupole-tandem mass spectrometrypesticide residuesdietary exposure assessmentfood safety index
spellingShingle Wei CHANG
Hui LI
Chunmei LI
Qiang HE
Zhan HUANG
Jiangtao CHEN
Pengyan LV
Meijie SONG
Qingsong LI
Hong LIU
Ao LI
Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in Chengdu
Shipin gongye ke-ji
quechers
gas chromatography-triple quadrupole-tandem mass spectrometry
pesticide residues
dietary exposure assessment
food safety index
title Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in Chengdu
title_full Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in Chengdu
title_fullStr Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in Chengdu
title_full_unstemmed Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in Chengdu
title_short Residue Levels and Chronic Dietary Intake Risk of Pesticide Residues in Fruits and Vegetables in Chengdu
title_sort residue levels and chronic dietary intake risk of pesticide residues in fruits and vegetables in chengdu
topic quechers
gas chromatography-triple quadrupole-tandem mass spectrometry
pesticide residues
dietary exposure assessment
food safety index
url http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021060041
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