Relaxation-compensated difference spin diffusion NMR for detecting 13C–13C long-range correlations in proteins and polysaccharides

The measurement of long-range distances remains a challenge in solid-state NMR structure determination of biological macromolecules. In 2D and 3D correlation spectra of uniformly 13C-labeled biomolecules, inter-residue, inter-segmental, and intermolecular 13C–13C cross peaks that provide important l...

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Bibliographic Details
Main Authors: Wang, Tuo, Williams, Jonathan Kyle, Schmidt-Rohr, Klaus, Hong, Mei
Other Authors: Massachusetts Institute of Technology. Department of Chemistry
Format: Article
Language:English
Published: Springer Netherlands 2016
Online Access:http://hdl.handle.net/1721.1/103054
https://orcid.org/0000-0002-7272-6885
https://orcid.org/0000-0002-1801-924X
https://orcid.org/0000-0001-5255-5858