Structural Insights into Bound Water in Crystalline Amino Acids: Experimental and Theoretical [superscript 17] O NMR

We demonstrate here that the [superscript 17]O NMR properties of bound water in a series of amino acids and dipeptides can be determined with a combination of nonspinning and magic-angle spinning experiments using a range of magnetic field strengths from 9.4 to 21.1 T. Furthermore, we propose a [sup...

Full description

Bibliographic Details
Main Authors: Craigen, Kimberley N., Wren, John E. C., Kroeker, Scott, Michaelis, Vladimir K., Keeler, Eric George, Ong, Ta-Chung, Penzel, Susanne, Griffin, Robert Guy
Other Authors: Massachusetts Institute of Technology. Department of Chemistry
Format: Article
Language:en_US
Published: American Chemical Society (ACS) 2017
Online Access:http://hdl.handle.net/1721.1/108242
https://orcid.org/0000-0002-6708-7660
https://orcid.org/0000-0003-1589-832X