3D MAS NMR Experiment Utilizing Through-Space

We demonstrate a novel 3D NNC magic angle spinning NMR experiment that generates ¹⁵N–¹⁵N internuclear contacts in protein systems using an optimized ¹⁵N–¹⁵N proton assisted recoupling (PAR) mixing period and a ¹³C dimension for improved resolution. The optimized PAR condition permits the acquisition...

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Bibliographic Details
Main Authors: Linse, Sara, Donovan, Kevin J, Silvers, Robert Paul Georg, Griffin, Robert Guy
Other Authors: Massachusetts Institute of Technology. Department of Chemistry
Format: Article
Language:en_US
Published: American Chemical Society (ACS) 2018
Online Access:http://hdl.handle.net/1721.1/114858
https://orcid.org/0000-0001-5830-6748
https://orcid.org/0000-0003-1589-832X