3D MAS NMR Experiment Utilizing Through-Space
We demonstrate a novel 3D NNC magic angle spinning NMR experiment that generates ¹⁵N–¹⁵N internuclear contacts in protein systems using an optimized ¹⁵N–¹⁵N proton assisted recoupling (PAR) mixing period and a ¹³C dimension for improved resolution. The optimized PAR condition permits the acquisition...
Main Authors: | , , , |
---|---|
Other Authors: | |
Format: | Article |
Language: | en_US |
Published: |
American Chemical Society (ACS)
2018
|
Online Access: | http://hdl.handle.net/1721.1/114858 https://orcid.org/0000-0001-5830-6748 https://orcid.org/0000-0003-1589-832X |