The benefits of energy-filtering in weak-beam microscopy

We have explored systematically the benefits of energy filtering to remove inelastically-scattered electrons with energy losses greater than about 10 eV from weak-beam images of dislocations. Digital weak-beam images were obtained of long dislocations in Ni3Ga using a Gatan Imaging Filter attached t...

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Main Authors: Jenkins, M, Martin, S, Hetherington, C, Kirk, M
Format: Conference item
Published: 2003
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author Jenkins, M
Martin, S
Hetherington, C
Kirk, M
author_facet Jenkins, M
Martin, S
Hetherington, C
Kirk, M
author_sort Jenkins, M
collection OXFORD
description We have explored systematically the benefits of energy filtering to remove inelastically-scattered electrons with energy losses greater than about 10 eV from weak-beam images of dislocations. Digital weak-beam images were obtained of long dislocations in Ni3Ga using a Gatan Imaging Filter attached to a Jeol 3000F FEGTEM. The image quality was assessed in terms of three parameters: the image peak width; the peak-to-background ratio; and the signal-to-noise ratio. All three of these measures were significantly improved in "zero-loss" energy-filtered images compared with unfiltered images taken under the same imaging conditions particularly in thick areas of foil (> 100 nm), where unfiltered images were badly degraded by chromatic aberration. In a foil of thickness similar to180nm energy-filtered images were of comparable quality to those obtainable in thin areas of foil (< 50 nm).
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spelling oxford-uuid:013d8101-4e62-46af-834d-28838210e6742022-03-26T08:33:48ZThe benefits of energy-filtering in weak-beam microscopyConference itemhttp://purl.org/coar/resource_type/c_5794uuid:013d8101-4e62-46af-834d-28838210e674Symplectic Elements at Oxford2003Jenkins, MMartin, SHetherington, CKirk, MWe have explored systematically the benefits of energy filtering to remove inelastically-scattered electrons with energy losses greater than about 10 eV from weak-beam images of dislocations. Digital weak-beam images were obtained of long dislocations in Ni3Ga using a Gatan Imaging Filter attached to a Jeol 3000F FEGTEM. The image quality was assessed in terms of three parameters: the image peak width; the peak-to-background ratio; and the signal-to-noise ratio. All three of these measures were significantly improved in "zero-loss" energy-filtered images compared with unfiltered images taken under the same imaging conditions particularly in thick areas of foil (> 100 nm), where unfiltered images were badly degraded by chromatic aberration. In a foil of thickness similar to180nm energy-filtered images were of comparable quality to those obtainable in thin areas of foil (< 50 nm).
spellingShingle Jenkins, M
Martin, S
Hetherington, C
Kirk, M
The benefits of energy-filtering in weak-beam microscopy
title The benefits of energy-filtering in weak-beam microscopy
title_full The benefits of energy-filtering in weak-beam microscopy
title_fullStr The benefits of energy-filtering in weak-beam microscopy
title_full_unstemmed The benefits of energy-filtering in weak-beam microscopy
title_short The benefits of energy-filtering in weak-beam microscopy
title_sort benefits of energy filtering in weak beam microscopy
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