Intergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysis

<p>Laue diffraction, energy scanning and reciprocal space mapping are three micro-beam synchrotron X-ray diffraction techniques allowing the investigation of local misorientation induced by the dislocation substructure. In this paper a comparison between the three methods is presented, based o...

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Main Authors: Hofmann, F, Abbey, B, Song, X, Dolbnya, I, Korsunsky, A
Format: Journal article
Language:English
Published: World Scientific Publishing Company 2010
Subjects:
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author Hofmann, F
Abbey, B
Song, X
Dolbnya, I
Korsunsky, A
author_facet Hofmann, F
Abbey, B
Song, X
Dolbnya, I
Korsunsky, A
author_sort Hofmann, F
collection OXFORD
description <p>Laue diffraction, energy scanning and reciprocal space mapping are three micro-beam synchrotron X-ray diffraction techniques allowing the investigation of local misorientation induced by the dislocation substructure. In this paper a comparison between the three methods is presented, based on the mapping of a single 311 reflection from a grain within a Ni polycrystal specimen deformed to a tensile plastic strain of ~9%. Qualitatively it is observed that the maps obtained by different techniques all share the same features, although some deviations exist due to experimental limitations associated with each of the measurement techniques.</p>
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spelling oxford-uuid:62e82e17-92ab-4426-9b41-77fd94ec84c22022-03-26T18:09:20ZIntergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysisJournal articlehttp://purl.org/coar/resource_type/c_dcae04bcuuid:62e82e17-92ab-4426-9b41-77fd94ec84c2Engineering & allied sciencesEnglishOxford University Research Archive - ValetWorld Scientific Publishing Company2010Hofmann, FAbbey, BSong, XDolbnya, IKorsunsky, A<p>Laue diffraction, energy scanning and reciprocal space mapping are three micro-beam synchrotron X-ray diffraction techniques allowing the investigation of local misorientation induced by the dislocation substructure. In this paper a comparison between the three methods is presented, based on the mapping of a single 311 reflection from a grain within a Ni polycrystal specimen deformed to a tensile plastic strain of ~9%. Qualitatively it is observed that the maps obtained by different techniques all share the same features, although some deviations exist due to experimental limitations associated with each of the measurement techniques.</p>
spellingShingle Engineering & allied sciences
Hofmann, F
Abbey, B
Song, X
Dolbnya, I
Korsunsky, A
Intergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysis
title Intergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysis
title_full Intergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysis
title_fullStr Intergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysis
title_full_unstemmed Intergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysis
title_short Intergranular lattice misorientation mapping by synchrotron x-ray micro-beams: Laue vs energy-resolved Laue vs monochromatic reciprocal space analysis
title_sort intergranular lattice misorientation mapping by synchrotron x ray micro beams laue vs energy resolved laue vs monochromatic reciprocal space analysis
topic Engineering & allied sciences
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AT abbeyb intergranularlatticemisorientationmappingbysynchrotronxraymicrobeamslauevsenergyresolvedlauevsmonochromaticreciprocalspaceanalysis
AT songx intergranularlatticemisorientationmappingbysynchrotronxraymicrobeamslauevsenergyresolvedlauevsmonochromaticreciprocalspaceanalysis
AT dolbnyai intergranularlatticemisorientationmappingbysynchrotronxraymicrobeamslauevsenergyresolvedlauevsmonochromaticreciprocalspaceanalysis
AT korsunskya intergranularlatticemisorientationmappingbysynchrotronxraymicrobeamslauevsenergyresolvedlauevsmonochromaticreciprocalspaceanalysis