Microanalysis at the atomic level

The optical arrangement of the high-resolution scanning transmission electron microscope (STEM) allows incoherent imaging conditions to be established simultaneously for both elastically and inelastically scattered electrons, with good detection efficiencies. For zone axis illumination and localized...

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Main Authors: Pennycook, S, Jesson, D, McGibbon, M, McGibbon, A, Nellist, P, Browning, N
Format: Conference item
Published: 1995
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author Pennycook, S
Jesson, D
McGibbon, M
McGibbon, A
Nellist, P
Browning, N
author_facet Pennycook, S
Jesson, D
McGibbon, M
McGibbon, A
Nellist, P
Browning, N
author_sort Pennycook, S
collection OXFORD
description The optical arrangement of the high-resolution scanning transmission electron microscope (STEM) allows incoherent imaging conditions to be established simultaneously for both elastically and inelastically scattered electrons, with good detection efficiencies. For zone axis illumination and localized inelastic transitions, both images show a resolution governed by the incident probe intensity profile, with maximum intensity occuring when the probe is located over the atomic columns. The high intensity elastic signal may therefore be used as an atomic resolution reference image for the low intensity inelastic signal, allowing spectroscopy to be achieved from selected atomic columns or planes. The potential of this approach in a 300-kV STEM is discussed.
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spelling oxford-uuid:e9850744-1d2c-49f6-ac3f-9956e3cb75792022-03-27T10:54:58ZMicroanalysis at the atomic levelConference itemhttp://purl.org/coar/resource_type/c_5794uuid:e9850744-1d2c-49f6-ac3f-9956e3cb7579Symplectic Elements at Oxford1995Pennycook, SJesson, DMcGibbon, MMcGibbon, ANellist, PBrowning, NThe optical arrangement of the high-resolution scanning transmission electron microscope (STEM) allows incoherent imaging conditions to be established simultaneously for both elastically and inelastically scattered electrons, with good detection efficiencies. For zone axis illumination and localized inelastic transitions, both images show a resolution governed by the incident probe intensity profile, with maximum intensity occuring when the probe is located over the atomic columns. The high intensity elastic signal may therefore be used as an atomic resolution reference image for the low intensity inelastic signal, allowing spectroscopy to be achieved from selected atomic columns or planes. The potential of this approach in a 300-kV STEM is discussed.
spellingShingle Pennycook, S
Jesson, D
McGibbon, M
McGibbon, A
Nellist, P
Browning, N
Microanalysis at the atomic level
title Microanalysis at the atomic level
title_full Microanalysis at the atomic level
title_fullStr Microanalysis at the atomic level
title_full_unstemmed Microanalysis at the atomic level
title_short Microanalysis at the atomic level
title_sort microanalysis at the atomic level
work_keys_str_mv AT pennycooks microanalysisattheatomiclevel
AT jessond microanalysisattheatomiclevel
AT mcgibbonm microanalysisattheatomiclevel
AT mcgibbona microanalysisattheatomiclevel
AT nellistp microanalysisattheatomiclevel
AT browningn microanalysisattheatomiclevel