Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity

Ananas comosus (L.) Merr is one of many commercially popular fruits in the cannery food industry that contributes to the increasingly mounting agro-industrial waste. In this study, a four−factor−three−level Box−Behnken design (BBD) that comprised of sonication time (A), solvent ratio (B), amplitude...

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Main Authors: Yahya, Nur Azzanizawaty, Abdul Wahab, Roswanira, Abdul Hamid, Mariani, Mahat, Naji Arafat, Mohamed Huri, Mohamad Afiq, Attan, Nursyafreena, Hashim, Siti Ernieyanti
Format: Article
Language:English
Published: Penerbit UTM Press 2020
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Online Access:http://eprints.utm.my/90000/1/RoswaniraAbWahab2020_StatisticalOptimizationandCharacterizationOfAcousticallyExtractedAnanas.pdf
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author Yahya, Nur Azzanizawaty
Abdul Wahab, Roswanira
Abdul Hamid, Mariani
Mahat, Naji Arafat
Mohamed Huri, Mohamad Afiq
Attan, Nursyafreena
Hashim, Siti Ernieyanti
author_facet Yahya, Nur Azzanizawaty
Abdul Wahab, Roswanira
Abdul Hamid, Mariani
Mahat, Naji Arafat
Mohamed Huri, Mohamad Afiq
Attan, Nursyafreena
Hashim, Siti Ernieyanti
author_sort Yahya, Nur Azzanizawaty
collection ePrints
description Ananas comosus (L.) Merr is one of many commercially popular fruits in the cannery food industry that contributes to the increasingly mounting agro-industrial waste. In this study, a four−factor−three−level Box−Behnken design (BBD) that comprised of sonication time (A), solvent ratio (B), amplitude (C) and liquid−solid ratio (D) for the ultrasound−assisted extraction (UAE) of pineapple peels (PP) was utilized to optimize the yield of total phenolic content (TPC). Under an optimized UAE condition [5 min; 50 % of ethanol: water; 65 % of amplitude; 35:1 mL/g of liquid−solid ratio], the highest TPC from PP of 708.10 mg gallic acid equivalent (GAE)/g DW was achieved. Antioxidant capacity analysis of PP revealed a high total flavonoid content (TFC) with the IC50 for 2,2−diphenyl−1−picrylhydrazyl (DPPH), and ferric reducing antioxidant power (FRAP) of 1146.86 ± 11.83 mg QE/g, 11.83 mg/mL and 1578.07 ± 25.96 µM Fe (II)/100g, respectively. High-performance liquid chromatography (HPLC) analysis revealed that the major flavonoid in the phenolic profile of PP extracts being catechin followed by quercetin and gallic acid. The UAE of PP extracts exhibited higher TPC than known conventional extraction techniques, thus indicating its efficacy to recover satisfactory quantities of phenolics in PP under optimized conditions.
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spelling utm.eprints-900002021-03-31T05:03:51Z http://eprints.utm.my/90000/ Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity Yahya, Nur Azzanizawaty Abdul Wahab, Roswanira Abdul Hamid, Mariani Mahat, Naji Arafat Mohamed Huri, Mohamad Afiq Attan, Nursyafreena Hashim, Siti Ernieyanti QD Chemistry Ananas comosus (L.) Merr is one of many commercially popular fruits in the cannery food industry that contributes to the increasingly mounting agro-industrial waste. In this study, a four−factor−three−level Box−Behnken design (BBD) that comprised of sonication time (A), solvent ratio (B), amplitude (C) and liquid−solid ratio (D) for the ultrasound−assisted extraction (UAE) of pineapple peels (PP) was utilized to optimize the yield of total phenolic content (TPC). Under an optimized UAE condition [5 min; 50 % of ethanol: water; 65 % of amplitude; 35:1 mL/g of liquid−solid ratio], the highest TPC from PP of 708.10 mg gallic acid equivalent (GAE)/g DW was achieved. Antioxidant capacity analysis of PP revealed a high total flavonoid content (TFC) with the IC50 for 2,2−diphenyl−1−picrylhydrazyl (DPPH), and ferric reducing antioxidant power (FRAP) of 1146.86 ± 11.83 mg QE/g, 11.83 mg/mL and 1578.07 ± 25.96 µM Fe (II)/100g, respectively. High-performance liquid chromatography (HPLC) analysis revealed that the major flavonoid in the phenolic profile of PP extracts being catechin followed by quercetin and gallic acid. The UAE of PP extracts exhibited higher TPC than known conventional extraction techniques, thus indicating its efficacy to recover satisfactory quantities of phenolics in PP under optimized conditions. Penerbit UTM Press 2020-07 Article PeerReviewed application/pdf en http://eprints.utm.my/90000/1/RoswaniraAbWahab2020_StatisticalOptimizationandCharacterizationOfAcousticallyExtractedAnanas.pdf Yahya, Nur Azzanizawaty and Abdul Wahab, Roswanira and Abdul Hamid, Mariani and Mahat, Naji Arafat and Mohamed Huri, Mohamad Afiq and Attan, Nursyafreena and Hashim, Siti Ernieyanti (2020) Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity. Jurnal Teknologi, 82 (4). pp. 1-10. ISSN 0127-9696 http://dx.doi.org/10.11113/jt.v82.14486
spellingShingle QD Chemistry
Yahya, Nur Azzanizawaty
Abdul Wahab, Roswanira
Abdul Hamid, Mariani
Mahat, Naji Arafat
Mohamed Huri, Mohamad Afiq
Attan, Nursyafreena
Hashim, Siti Ernieyanti
Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity
title Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity
title_full Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity
title_fullStr Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity
title_full_unstemmed Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity
title_short Statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity
title_sort statistical optimization and characterization of acoustically extracted ananas comosus peel powder with enhanced antioxidant capacity
topic QD Chemistry
url http://eprints.utm.my/90000/1/RoswaniraAbWahab2020_StatisticalOptimizationandCharacterizationOfAcousticallyExtractedAnanas.pdf
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